Chapter9 Non-destructive Examination of Multiphase Material Distribution in Uranium Hexafluoride Cylinders Using Steady-State Laser Doppler Vibrometery David Goodman, Kelly Rowland, Sheriden Smith, Karen Miller, and Eric Flynn Abstract The ability to detect the diversion of a significant quantity of nuclear material is the objective of international nuclear safeguards, and safeguarding uranium enrichment technology is especially important in preventing the spread of nuclear weapons. In gas centrifuge enrichment plants, the uranium is in the form of uranium hexafluoride (UF6), which regularly transitions between phases during processing and storage due to its low triple point. The variation of material distribution in Uf6 cylinders has a significant effect on enrichment measurement uncertainty, especially with increasing accuracy of passive neutron assay measurements, motivating interest in non-destructive methods of examining UF6 cylinder fill distributions. For this study, a novel steady-state scanning laser Doppler vibrometer (LDV) system is used to determine the material and phase distributions within small UF6 cylinders. This technology induces steady-state ultrasonic waves throughout an object and then uses a scanning laser to measure vibrational wavenumber at pixilated points on the object. Different materials and phases are excited by the ultrasonic waves to different extents, changing the local measured wavenumbers and allowing fill distributions of the storage cylinders to be mapped. Through non-destructive examination of the variation in typical fill profiles of UF6 cylinders, the uncertainty associated with neutron measurements of UF6 cylinders may be better characterized. Keywords Ultrasound • Non-destructive evaluation • Scanning laser Doppler vibrometer • Uranium hexafluoride • Nuclear safeguards 9.1 Introduction The purpose of this study is to test whether a steady-state scanning laser Doppler vibrometer (LDV) system can be used to characterize the fill profile of uranium hexafluoride (UF6) inside storage cylinders. The ability to detect the diversion of a significant quantity of nuclear material is the objective of international nuclear safeguards, and safeguarding uranium D. Goodman Department of Nuclear Engineering, University of Michigan, Ann Arbor, MI 48109, USA e-mail: digoodma@umich.edu K. Rowland Department of Nuclear Engineering, University of California, Berkeley, CA 94704, USA e-mail: rowlak@rpi.edu S. Smith Department of Mechanical Engineering, Colorado State University, Fort Collins, CO 80523, USA e-mail: Sheriden@rams.colostate.edu K.Miller Safeguards Science & Technology Group, Los Alamos National Laboratory, Los Alamos, NM 87545, USA e-mail: kamiller@lanl.gov E. Flynn ( ) Engineering Institute, Los Alamos National Laboratory, Los Alamos, NM 87545, USA e-mail: eflynn@lanl.gov A. Wicks (ed.), Structural Health Monitoring, Volume 5: Proceedings of the 32nd IMAC, A Conference and Exposition on Structural Dynamics, 2014, Conference Proceedings of the Society for Experimental Mechanics Series, DOI 10.1007/978-3-319-04570-2__9, © The Society for Experimental Mechanics, Inc. 2014 81
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